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63,64 The experimental technique involves subjecting nitrogen gas and the chalcogen vapour to a microwave discharge in an argon atmosphere. The products are trapped in the argon matrix at 12 K and, with the aid of isotopic substitution (15N, 34 S, 76 Se and 80Se), the IR and Raman spectra can be assigned to specific molecules. 3). The strongest absorptions are observed for the antisymmetric stretching vibration of the ENE species (E = S, 1225 cm-1; E = Se, 1021 cm-1). 5°, respectively.

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